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Riley, T. (2025). Geochemical and geochronological data from the Drygalski Fjord region of South Georgia (Version 1.0) [Data set]. NERC EDS UK Polar Data Centre. https://doi.org/10.5285/270714e6-f141-4c01-8a13-2bdfaca80ced</gco:CharacterString>
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Analytical methods&#xD;
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University College London&#xD;
Zircon U-Pb geochronology used laser ablation inductively coupled mass spectrometry (LA-ICP-MS) facilities (Agilent 7700 coupled to a New Wave Research 193 nm excimer laser) at the London Geochronology Centre based in University College London. Heavy minerals were separated from bulk sediment samples using standard density liquid and magnetic separation procedures. Zircon-enriched extracts were mounted in hard epoxy resin on glass slides and polished for analysis. Typical laser spot sizes of 25 mircometers were used with a 7-10 Hz repetition rate and a fluence of 2.5 J/cm2. Background measurement before ablation lasted 15 seconds and laser ablation dwell time was 25 seconds.The external zircon standard was Plesovice,which has a TIMS reference age 337.13 +/- 0.37 Ma (Slama et al., 2008). Standard errors on isotope ratios and ages include the standard deviation of 206Pb/238U ages of the Plesovice standard zircon. Time-resolved signals that record isotopic ratios with depth in each crystal were processed using GLITTER 4.5, data reduction software, developed by the ARC National Key Centre for Geochemical Evolution and Metallogeny of Continents (GEMOC) at Macquarie University and CSIRO Exploration and Mining. Processing enabled filtering to remove spurious signals owing to overgrowth boundaries, weathering, inclusions, or fractures.&#xD;
NordSIMS analytical facility (Stockholm)&#xD;
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Lu-Hf isotope analysis&#xD;
Isotope analyses were carried out at NIGL using a Thermo Scientific Neptune Plus MC-ICP-MS coupled to a New Wave Research UP193UC Excimer laser ablation system. Helium was used as the carrier gas through the ablation cell with Ar make-up gas being connected via a T-piece and sourced from a Cet...(17)
Data quality: 
U-Pb ages were calculated using the 206Pb/238U ratios for samples dated as &amp;lt;1.1 Ga, and the 207Pb/206Pb ratios was used for older grains. Discordance was determined using (207Pb/235U - 206Pb/238U) / 206Pb/238U) and similar for 207Pb/206Pb ages. &#xD;
Lu_Hf analytical uncertainties for unknowns were propagated by quadratic addition to include the standard error of the mean of the analysis and the reproducibility of the 91500 reference material. epsilonHf values were calculated using a 176Lu decay constant of 1.867 x 10-11y-1 (S&amp;ouml;derlund et al., 2004), the present-day chondritic 176Lu/177Hf value of 0.0336 and 176Hf/177Hf ratio of 0.282785 (Bouvier et al., 2008).</gco:CharacterString>
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